Synthesis process of thiol || Advance organic synthesis Method

 Synthesis process of thiol (RSH):-

 Synthesis process of thiol (RSH):-

                                                               In this method Required material 

1) Two stand 

2) Two Round bottom flask 

3) One Connecting Tube

4) FeS ( Metal)

5) Salfuric acid 

6) Alkyl halides 

7) Sodium hydroxide 

8) Injunction Nogal 

9) Round bottom Nogal Closing Rubber 

Safety Guidelines are available in the given images and this post is only for Educational purposes.

Safety Guidelines:-

1) salfuric acid is dangerous for touch.

2) Hydrogen salfide gass is toxic. 

3) Sodium hydroxide is flammable.

Stap By stap Complicated the reaction.

Step 1:- Febric salfide metal add in the round bottom flask and close the 

Head.

Step 2:- Connecting the second round bottom flask with connecting tube.

Step 3:- Tested that Not any linkages are present in the round bottom flask connecting method.

Step 4:- Alkyl halides and sodium hydroxide mixture taken in the second round bottom flask and close totaly with the help of Round bottom Nogal Closing Rubber.

Step 5:- Drop and Drop add salfuric acid in the round bottom flask, with the help of injection Nogal.

Reaction is given in the digram.